In this paper are described sampling procedures, preparation of samples for analysis, measurements and measurement results for soil samples in the area of Parish Krašić, coffee and tea cups used by blessed Cardinal Stepinac before he died and metal sheets of coffin in which Cardinal was lying to the transfer of remains in the Zagreb Cathedral. By analyzing the measured spectra of characteristic x-rays obtained from the samples, it was found that the metal sheets contain zinc with lead additives, while the antimony is traced. The results of the measurement of antimony concentration in the sheets samples are in the MDL-356 ppm. Fast neutron activation analysis was used to determine the chemical composition of coffee and tea cups as well as metal sheets. The gamma-ray coffee cup spectrum indicates the presence of radioactive thorium. By using the direct comparison method it was estimated 24 ppm of Th in the coffee cup. By using the radioactive 241Am it was shown that the black pigment coffee cup contains Ag. Tea cup glass contains higher Ba concentrations, but Sb is not measured in any cup. Antimony in the soil was present in the interval 0-2.9 ppm. The concentrations of the elements in the soil samples were determined: K (1,18-1,63%), Ca (0,44-6,09%), Ti (5725-7806 ppm), V (120,8-224,9 ppm), Cr (44,8-170,6 ppm), Mn ( 441,1-1315,1 ppm), Fe (3,1-6,4%), Ni (52,6-264,0 ppm), Cu (20,2-149,0 ppm), Zn (126,7-442,8 ppm), Ga (19,4-30,4 ppm), As (7,5-17,8 ppm), Br (57,0-176,0 ppm) Rb (76,6-166,2 ppm), Sr (73,7-141,8 ppm) Y (27,3-63,2 ppm) Zr (201,2-470,7 ppm) and Pb (17,9-76,2 ppm). The concentration values of all 18 elements are within normal values.